Sodium Iodide → HCID 10966432, compound

HRID 744104Notes

Reaction equation

HRID 744104 reaction equation
[OH:1][C:2]1[CH:14]=[CH:13][C:5](/[CH:6]=[CH:7]/[C:8]([O:10][CH2:11][CH3:12])=[O:9])=[CH:4][CH:3]=1.[CH2:15](I)[CH2:16][CH3:17].[I-].[Na+]>>[CH2:15]([O:1][C:2]1[CH:3]=[CH:4][C:5](/[CH:6]=[CH:7]/[C:8]([O:10][CH2:11][CH3:12])=[O:9])=[CH:13][CH:14]=1)[CH2:16][CH3:17]

Participants

4

Reactant 3

HCID 5238Sodium IodideHCID 336431-IodopropaneHCID 676946p-Coumaric acid ethyl ester

Product 1

HCID 10966432HCID 10966432, compoundYield 93.9%

Procedure

Following a procedure similar to that described in Preparation 115, but using 9.61 g of ethyl (E)-p-hydroxycinnamate and 10.20 g of propyl iodide and not using sodium iodide, 11.00 g of the title compound were obtained as a solid material.

Workup

  1. customthat described in Preparation 115

Sources & evidence

ORD record
ord-89f170b3d5754b698dcbd24ca4e49d0b
Source dataset
uspto-grants-1996_09
Patent number
US05559109

Reaction notes

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