Water → 1142-15-0

HRID 745287Notes

Reaction equation

HRID 745287 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[CH:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:4][CH:3]=1.[C:16]([O-])([O-])=O.[K+].[K+].CI.O>CN(C)C=O.C(Cl)Cl>[CH3:16][O:1][C:2]1[CH:3]=[CH:4][C:5]([CH:8]=[CH:9][C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=2)=[CH:6][CH:7]=1

Participants

7

Reactant 4

HCID 962WaterHCID 6328Methyl iodideHCID 11430Potassium CarbonateHCID 929714-Hydroxystilbene

Product 1

HCID 143591142-15-0

Reagents, catalysts & solvents 2

HCID 6228DimethylformamideSolventHCID 6344DichloromethaneSolvent

Procedure

19.6 grams (0.1 mole) of 4-hydroxystilbene, 135 grams of K2CO3 and 135 grams of methyl iodide were stirred in 500 ml of dimethyl-formamide for 20 hours at room temperature. After dilution with water the mixture was shaken with methylene chloride.

Sources & evidence

ORD record
ord-8e2659047aec4f36b90b44ce9544afee
Source dataset
uspto-grants-1986_07
Patent number
US04598091

Reaction notes

Loading…