反应详情

Into 40 ml of distilled trifluoroacetic acid was dissolved 1.0 g of palladium acetate. The solvent was distilled off and an additional 20 ml of trifluoroacetic acid was added and distilled off. The residual solid was dried in facuo at 40° C. to afford 1.3 g of brown product, i.e. palladium (II) trifluoroacetate, mp 210° C. (dec).

1. distillationThe solvent was distilled off
2. additionan additional 20 ml of trifluoroacetic acid was added
3. distillationdistilled off
4. customThe residual solid was dried in facuo at 40° C.