Hydrochloric Acid → 1159010-32-8

HRID 74570Notes

Reaction equation

HRID 74570 reaction equation
[H][H].[CH3:3][CH:4]1[CH2:13][CH:12]2[CH:7]([CH2:8][CH2:9][CH2:10][CH2:11]2)[NH:6][CH2:5]1.[ClH:14]>CO.[Pt](=O)=O>[ClH:14].[CH3:3][CH:4]1[CH2:13][CH:12]2[CH:7]([CH2:8][CH2:9][CH2:10][CH2:11]2)[NH:6][CH2:5]1

Participants

6

Reactant 3

HCID 313Hydrochloric AcidHCID 155554733-Methyl-decahydroquinolineHCID 178418361HCID 178418361, compound

Product 1

HCID 673377491159010-32-8

Reagents, catalysts & solvents 2

HCID 345198Adams' catalystCatalystHCID 887MethanolSolvent

Procedure

In a hydrogen atmosphere 500 mg (3.5 mmol) 3-methyl-decahydro-quinoline, 75 mg platinum dioxide in 50 mL methanol and 3.5 mL 1M aqueous hydrochloric acid solution were hydrogenated at RT and 50 psi for 4 h. After removal of the catalyst by suction filtering the reaction mixture was evaporated down.

Workup

  1. customwere hydrogenated at RT
  2. customAfter removal of the catalyst by suction
  3. filtrationfiltering the reaction mixture
  4. customwas evaporated down

Sources & evidence

ORD record
ord-b45247443a5b4997ad16ef0306794e9c
Source dataset
uspto-grants-2014_09
Patent number
US08829006B2

Reaction notes

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