HRID74570

反应详情

EQUATION

反应方程式

HRID 74570 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

In a hydrogen atmosphere 500 mg (3.5 mmol) 3-methyl-decahydro-quinoline, 75 mg platinum dioxide in 50 mL methanol and 3.5 mL 1M aqueous hydrochloric acid solution were hydrogenated at RT and 50 psi for 4 h. After removal of the catalyst by suction filtering the reaction mixture was evaporated down.

WORKUP

后处理

  1. customwere hydrogenated at RT
  2. customAfter removal of the catalyst by suction
  3. filtrationfiltering the reaction mixture
  4. customwas evaporated down