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HRID747391

反应详情

EQUATION

反应方程式

HRID 747391 的结构方程式

REACTANTS

反应物

4
结构：CN
HCID6329

Methylamine

CH5N

结构：CCN
HCID6341

Ethanamine

C2H7N

结构：C#CC(C)(C)N
HCID76319

3-Butyn-2-amine, 2-methyl-

C5H9N

结构：O=S(=O)(Cl)Cc1ccc(Cl)cc1
HCID227304

(4-Chlorophenyl)methanesulfonyl chloride

C7H6Cl2O2S

PRODUCTS

生成物

1
结构：CNCC1=C(c2ccc(Cl)cc2)S(=O)(=O)NC1(C)C
HCID17973783

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from (4-chlorophenyl)methanesulfonyl chloride and 1,1-dimethylpropargylamine according to the procedure described for Intermediate 4 replacing ethylamine by methylamine in the last step. 1H-NMR (DMSO-d6) δ 7.72 (bs, 1 H), 7.53 (m, 4H), 3.33 (s, 2 H), 2.16 (s, 3 H), 1.45 (s, 6 H).