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HRID751183

反应详情

EQUATION

反应方程式

HRID 751183 的结构方程式

REACTANTS

反应物

4
结构：CN(C)C(=O)N=NC(=O)N(C)C
HCID4278

N,N,N′,N′-Tetramethylazodicarboxamide

C6H12N4O2

结构：CCCCP(CCCC)CCCC
HCID13831

Tributylphosphine

C12H27P

结构：CCOC(=O)Cn1ccc2ccc(O)cc21
HCID68821422

(6-Hydroxy-indol-1-yl)-acetic acid ethyl ester

C12H13NO3

结构：OCCCC#Cc1cccc(OC(F)(F)F)c1
HCID68821693

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)Cn1ccc2ccc(OCCCC#Cc3cccc(OC(F)(F)F)c3)cc21
HCID68822183

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described for example 1 d], (6-hydroxy-indol-1-yl)-acetic acid ethyl ester (example 1 c]) was reacted with 5-(3-trifluoromethoxy-phenyl)-pent-4-yn-1-ol in the presence of N,N,N′,N′-tetramethyl azodicarboxamide and tributylphosphine to give the title compound as colorless oil.

WORKUP

后处理

  1. customdescribed for example 1 d