HRID77509

反应详情

EQUATION

反应方程式

HRID 77509 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 60 mg (S)-{1-[(4-Chloro-benzylcarbamoyl)-methyl]-piperidin-3-yl}-carbamic acid tert-butyl ester (intermediate 7.7A) in 5 ml dichloromethane is treated with 50 μl TFA and stirred overnight at room temperature. The mixture is evaporated to yield the title compound as a trifluoroacetate.

WORKUP

后处理

  1. customThe mixture is evaporated