Dimethyl Sulfoxide → 5,5-Dimethyl-1,3-dioxane-2-propionaldehyde

HRID 799209Notes

Reaction equation

HRID 799209 reaction equation
[CH2:30]([Cl:31])[Cl:32].[CH3:11][C:12]1([CH3:22])[CH2:13][O:14][CH:15]([CH2:18][CH2:19][CH2:20][OH:21])[O:16][CH2:17]1.[CH3:1][S:2]([CH3:3])=[O:4].[CH3:23][CH2:24][N:25]([CH2:26][CH3:27])[CH2:28][CH3:29].[Cl:5][C:6]([C:7]([Cl:8])=[O:9])=[O:10]>>[CH3:11][C:12]1([CH3:22])[CH2:13][O:14][CH:15]([CH2:18][CH2:19][CH:20]=[O:21])[O:16][CH2:17]1

Participants

6

Reactant 5

HCID 679Dimethyl SulfoxideHCID 6344DichloromethaneHCID 8471TriethylamineHCID 65578Oxalyl chlorideHCID 108211213-(5,5-Dimethyl-1,3-dioxan-2-yl)-1-propanol

Product 1

HCID 938825,5-Dimethyl-1,3-dioxane-2-propionaldehyde

Sources & evidence

ORD record
ord-98849a3a9d3e48c78c7bda935377a396
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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