Ammonium → Tert-butyl 4-azido-5-hydroxyazepane-1-carboxylate

HRID 805812Notes

Reaction equation

HRID 805812 reaction equation
[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH2:10][CH:11]2[O:12][CH:13]2[CH2:14][CH2:15]1.[CH3:16][CH2:17][OH:18].[Cl-:19].[N-:22]=[N+:23]=[N-:24].[NH4+:20].[Na+:21].[OH2:25]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH2:10][CH:11]([N:22]=[N+:23]=[N-:24])[CH:13]([OH:12])[CH2:14][CH2:15]1

Participants

8

Reactant 7

HCID 223AmmoniumHCID 312ChlorideHCID 702EthanolHCID 923Sodium ionHCID 962WaterHCID 33558AzideHCID 58717040Tert-butyl 8-oxa-4-azabicyclo[5.1.0]octane-4-carboxylate

Product 1

HCID 58717042Tert-butyl 4-azido-5-hydroxyazepane-1-carboxylate

Sources & evidence

ORD record
ord-55568ed8e0e04abf9d0b01721b17a7f8
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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