Dimethyl Sulfoxide → Benzyl (4-oxocyclohexyl)carbamate

HRID 808761Notes

Reaction equation

HRID 808761 reaction equation
[CH2:11]([c:12]1[cH:13][cH:14][cH:15][cH:16][cH:17]1)[O:18][C:19]([NH:20][CH:21]1[CH2:22][CH2:23][CH:24]([OH:27])[CH2:25][CH2:26]1)=[O:28].[CH3:29][CH2:30][N:31]([CH2:32][CH3:33])[CH2:34][CH3:35].[CH3:7][S:8]([CH3:9])=[O:10].[Cl:1][C:2]([C:3]([Cl:4])=[O:5])=[O:6].[Cl:36][CH2:37][Cl:38]>>[CH2:11]([c:12]1[cH:13][cH:14][cH:15][cH:16][cH:17]1)[O:18][C:19]([NH:20][CH:21]1[CH2:22][CH2:23][C:24](=[O:27])[CH2:25][CH2:26]1)=[O:28]

Participants

6

Reactant 5

HCID 679Dimethyl SulfoxideHCID 6344DichloromethaneHCID 8471TriethylamineHCID 65578Oxalyl chlorideHCID 51750654-(Z-amino)cyclohexanol

Product 1

HCID 14615292Benzyl (4-oxocyclohexyl)carbamate

Sources & evidence

ORD record
ord-745ade360fab402b95df34217ea1f97f
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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