HRID81344

反应详情

EQUATION

反应方程式

HRID 81344 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2-methyl-3-methylene-7-nitro-2,3-dihydro-isoindol-1-one (13.96 g) is suspended in THF and mixed with a spatula tip of Pd/C (5%) and hydrogenated under H2 pressure (3 bar). For working up the catalyst is filtered off and the solvent is eliminated in vacuo.

WORKUP

后处理

  1. filtrationis filtered off