HRID81344
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
2-methyl-3-methylene-7-nitro-2,3-dihydro-isoindol-1-one (13.96 g) is suspended in THF and mixed with a spatula tip of Pd/C (5%) and hydrogenated under H2 pressure (3 bar). For working up the catalyst is filtered off and the solvent is eliminated in vacuo.
WORKUP
后处理
- filtrationis filtered off