Dimethylformamide → 5-Nitro-3-chloro-2,4-difluorobenzoyl chloride

HRID 813821Notes

Reaction equation

HRID 813821 reaction equation
[Cl:16][C:17]([C:18]([Cl:19])=[O:20])=[O:21].[Cl:27][CH2:28][Cl:29].[N+:1](=[O:2])([O-:3])[c:4]1[c:5]([F:15])[c:6]([Cl:14])[c:7]([F:13])[c:8]([C:9](=[O:10])[OH:11])[cH:12]1.[O:22]=[CH:23][N:24]([CH3:25])[CH3:26]>>[N+:1](=[O:2])([O-:3])[c:4]1[c:5]([F:15])[c:6]([Cl:14])[c:7]([F:13])[c:8]([C:9](=[O:10])[Cl:16])[cH:12]1

Participants

5

Reactant 4

HCID 6228DimethylformamideHCID 6344DichloromethaneHCID 65578Oxalyl chlorideHCID 155499183-Chloro-2,4-difluoro-5-nitrobenzoic acid

Product 1

HCID 155499195-Nitro-3-chloro-2,4-difluorobenzoyl chloride

Sources & evidence

ORD record
ord-904a88512b684dd18c60b44ede83d521
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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