Ammonium → Ethyl 4-amino-3-(2,4-difluorophenylthio)benzoate

HRID 814263Notes

Reaction equation

HRID 814263 reaction equation
[CH3:26][CH2:27][OH:28].[Cl-:24].[F:1][c:2]1[c:3]([S:9][c:10]2[cH:11][c:12]([C:13](=[O:14])[O:15][CH2:16][CH3:17])[cH:18][cH:19][c:20]2[N+:21]([O-:22])=[O:23])[cH:4][cH:5][c:6]([F:8])[cH:7]1.[Fe:30].[NH4+:25].[OH2:29]>>[F:1][c:2]1[c:3]([S:9][c:10]2[cH:11][c:12]([C:13](=[O:14])[O:15][CH2:16][CH3:17])[cH:18][cH:19][c:20]2[NH2:21])[cH:4][cH:5][c:6]([F:8])[cH:7]1

Participants

7

Reactant 6

HCID 223AmmoniumHCID 312ChlorideHCID 702EthanolHCID 962WaterHCID 23925IronHCID 10359815Ethyl 3-(2,4-difluorophenylthio)-4-nitrobenzoate

Product 1

HCID 10040979Ethyl 4-amino-3-(2,4-difluorophenylthio)benzoate

Sources & evidence

ORD record
ord-2ffa14b4088e43dabca0bbce258ebe13
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

Loading…