Dimethylformamide → 5-tert-Butyl-2-(4-ethynylphenyl)-1,3-dithiane

HRID 817123Notes

Reaction equation

HRID 817123 reaction equation
[C:11]([CH3:12])([CH3:13])([CH3:14])[CH:15]([CH2:16][SH:17])[CH2:18][SH:19].[C:1](#[CH:2])[c:3]1[cH:4][cH:5][c:6]([CH:7]=[O:8])[cH:9][cH:10]1.[CH2:32]([Cl:33])[Cl:34].[CH3:20][N:21]([CH3:22])[CH:23]=[O:24].[CH3:25][O:26][S:27]([O:28][CH3:29])(=[O:30])=[O:31].[CH3:35][CH2:36][N:37]([CH2:38][CH3:39])[CH2:40][CH3:41]>>[C:1](#[CH:2])[c:3]1[cH:4][cH:5][c:6]([CH:7]2[S:17][CH2:16][CH:15]([C:11]([CH3:12])([CH3:13])[CH3:14])[CH2:18][S:19]2)[cH:9][cH:10]1

Participants

7

Reactant 6

HCID 6228DimethylformamideHCID 6344DichloromethaneHCID 6497Dimethyl SulfateHCID 8471TriethylamineHCID 27716454-EthynylbenzaldehydeHCID 149804272-tert-Butylpropane-1,3-dithiol

Product 1

HCID 224210215-tert-Butyl-2-(4-ethynylphenyl)-1,3-dithiane

Sources & evidence

ORD record
ord-d7637cabb13344d388a38300c28fc547
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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