Ethylene Glycol → N-methyl-N-1,3-dioxolan-2-ylmethyl-2,6-dinitro-4-trifluoromethylaniline

HRID 821564Notes

Reaction equation

HRID 821564 reaction equation
[CH3:1][N:2]([c:3]1[c:4]([N+:16](=[O:17])[O-:18])[cH:5][c:6]([C:12]([F:13])([F:14])[F:15])[cH:7][c:8]1[N+:9](=[O:10])[O-:11])[CH2:19][CH:20]([O:21][CH3:22])[O:23][CH3:24].[CH3:40][CH2:41][O:42][C:43](=[O:44])[CH3:45].[OH:25][CH2:26][CH2:27][OH:28].[c:29]1([CH3:30])[cH:31][cH:32][c:33]([S:34]([OH:35])(=[O:36])=[O:37])[cH:38][cH:39]1>>[CH3:1][N:2]([c:3]1[c:4]([N+:16](=[O:17])[O-:18])[cH:5][c:6]([C:12]([F:13])([F:14])[F:15])[cH:7][c:8]1[N+:9](=[O:10])[O-:11])[CH2:19][CH:20]1[O:21][CH2:22][CH2:24][O:23]1

Participants

5

Reactant 4

HCID 174Ethylene GlycolHCID 6101p-Toluenesulfonic acidHCID 8857Ethyl AcetateHCID 20492553N-Methyl-N-(2,2-dimethoxyethyl)-2,6-dinitro-4-trifluoromethylaniline

Product 1

HCID 13175524N-methyl-N-1,3-dioxolan-2-ylmethyl-2,6-dinitro-4-trifluoromethylaniline

Sources & evidence

ORD record
ord-2b590355ef3c4457935ab2ba10532fc3
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

Loading…