Acetate → 2-(1,3-Dioxolan-2-yl)-4-methoxyaniline

HRID 822584Notes

Reaction equation

HRID 822584 reaction equation
[C:20]([O-:21])(=[O:22])[CH3:23].[CH3:1][O:2][c:3]1[cH:4][cH:5][c:6]([N+:14]([O-:15])=[O:16])[c:7]([CH:9]2[O:10][CH2:11][CH2:12][O:13]2)[cH:8]1.[CH3:25][CH2:26][O:27][C:28](=[O:29])[CH3:30].[Na+:24].[OH2:17].[OH2:18].[OH2:19].[Pt:31](=[O:32])=[O:33]>>[CH3:1][O:2][c:3]1[cH:4][cH:5][c:6]([NH2:14])[c:7]([CH:9]2[O:10][CH2:11][CH2:12][O:13]2)[cH:8]1

Participants

7

Reactant 6

HCID 175AcetateHCID 923Sodium ionHCID 962Water3×HCID 8857Ethyl AcetateHCID 345198Adams' catalystHCID 572490272-(5-Methoxy-2-nitrophenyl)-1,3-dioxolane

Product 1

HCID 153389082-(1,3-Dioxolan-2-yl)-4-methoxyaniline

Sources & evidence

ORD record
ord-a5db8d1da5c14a56b6229aca4ace9b83
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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