Dimethylformamide → ethyl 5-chloro-3-(chlorosulfonyl)-1-(phenylsulfonyl)-1H-indole-2-carboxylate

HRID 828658Notes

Reaction equation

HRID 828658 reaction equation
[CH3:35][N:36]([CH3:37])[CH:38]=[O:39].[Cl:1][c:2]1[cH:3][c:4]2[c:5]([S:25](=[O:26])(=[O:27])[OH:28])[c:6]([C:20](=[O:21])[O:22][CH2:23][CH3:24])[n:7]([S:11](=[O:12])(=[O:13])[c:14]3[cH:15][cH:16][cH:17][cH:18][cH:19]3)[c:8]2[cH:9][cH:10]1.[Cl:29][C:30]([C:31]([Cl:32])=[O:33])=[O:34].[Cl:40][CH2:41][Cl:42]>>[Cl:1][c:2]1[cH:3][c:4]2[c:5]([S:25](=[O:26])(=[O:28])[Cl:29])[c:6]([C:20](=[O:21])[O:22][CH2:23][CH3:24])[n:7]([S:11](=[O:12])(=[O:13])[c:14]3[cH:15][cH:16][cH:17][cH:18][cH:19]3)[c:8]2[cH:9][cH:10]1

Participants

5

Reactant 4

HCID 6228DimethylformamideHCID 6344DichloromethaneHCID 65578Oxalyl chlorideHCID 224015045-Chloro-2-(ethoxycarbonyl)-1-(phenylsulfonyl)-1H-indole-3-sulfonic acid

Product 1

HCID 22401482ethyl 5-chloro-3-(chlorosulfonyl)-1-(phenylsulfonyl)-1H-indole-2-carboxylate

Sources & evidence

ORD record
ord-94320eab1b334cd69fc2f8a80c591b65
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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