Methane → Rac-ethyl (1s,4s)-4-(methanesulfonyloxy)cyclohexane-1-carboxylate

HRID 828857Notes

Reaction equation

HRID 828857 reaction equation
[CH2:1]([CH3:2])[O:3][C:4](=[O:5])[CH:6]1[CH2:7][CH2:8][CH:9]([OH:12])[CH2:10][CH2:11]1.[CH3:13][CH2:14][N:15]([CH2:16][CH3:17])[CH2:18][CH3:19].[CH4:25].[Cl:26][CH2:27][Cl:28].[S:20](=[O:21])(=[O:22])([Cl:23])[Cl:24]>>[CH2:1]([CH3:2])[O:3][C:4](=[O:5])[CH:6]1[CH2:7][CH2:8][CH:9]([O:12][S:20](=[O:21])(=[O:22])[CH3:25])[CH2:10][CH2:11]1

Participants

6

Reactant 5

HCID 297MethaneHCID 6344DichloromethaneHCID 8471TriethylamineHCID 24648Sulfuryl chlorideHCID 86973Ethyl 4-hydroxycyclohexanecarboxylate

Product 1

HCID 58812756Rac-ethyl (1s,4s)-4-(methanesulfonyloxy)cyclohexane-1-carboxylate

Sources & evidence

ORD record
ord-d8fb9613c1544cabaf3e445a81370931
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

Loading…