Sodium ion → 6-Bromo-1-methyl-1,4-dihydro-pyrido[2,3-d][1,3]oxazin-2-one

HRID 829146Notes

Reaction equation

HRID 829146 reaction equation
[Br:1][c:2]1[cH:3][c:4]2[c:5]([n:11][cH:12]1)[NH:6][C:7](=[O:10])[O:8][CH2:9]2.[CH3:22][CH2:23][O:24][C:25]([CH3:26])=[O:27].[H-:13].[I:15][CH3:16].[Na+:14].[O:17]=[CH:18][N:19]([CH3:20])[CH3:21]>>[Br:1][c:2]1[cH:3][c:4]2[c:5]([n:11][cH:12]1)[N:6]([CH3:16])[C:7](=[O:10])[O:8][CH2:9]2

Participants

7

Reactant 6

HCID 923Sodium ionHCID 6228DimethylformamideHCID 6328Methyl iodideHCID 8857Ethyl AcetateHCID 166653HydrideHCID 159259906-bromo-1H,2H,4H-pyrido(2,3-d)(1,3)oxazin-2-one

Product 1

HCID 596197196-Bromo-1-methyl-1,4-dihydro-pyrido[2,3-d][1,3]oxazin-2-one

Sources & evidence

ORD record
ord-3690b2e799b04a83a0422b80c9edc7c2
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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