Ammonium → benzyl N-(4-hydroxy-4-methylcyclohexyl)carbamate

HRID 835105Notes

Reaction equation

HRID 835105 reaction equation
[CH3:32][CH2:33][O:34][CH2:35][CH3:36].[Ce+3:20].[Cl-:19].[Cl-:21].[Cl-:22].[Cl-:25].[Li:23][CH3:24].[NH4+:26].[O:1]=[C:2]1[CH2:3][CH2:4][CH:5]([NH:8][C:9]([O:10][CH2:11][c:12]2[cH:13][cH:14][cH:15][cH:16][cH:17]2)=[O:18])[CH2:6][CH2:7]1.[O:27]1[CH2:28][CH2:29][CH2:30][CH2:31]1>>[OH:1][C:2]1([CH3:24])[CH2:3][CH2:4][CH:5]([NH:8][C:9]([O:10][CH2:11][c:12]2[cH:13][cH:14][cH:15][cH:16][cH:17]2)=[O:18])[CH2:6][CH2:7]1

Participants

8

Reactant 7

HCID 223AmmoniumHCID 312Chloride4×HCID 3283Diethyl EtherHCID 8028TetrahydrofuranHCID 114853Cerium(3+)HCID 14615292Benzyl (4-oxocyclohexyl)carbamateHCID 178418348HCID 178418348, compound

Product 1

HCID 71231539benzyl N-(4-hydroxy-4-methylcyclohexyl)carbamate

Sources & evidence

ORD record
ord-d0297abae8524157bf76752472936c74
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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