huagongshe.com
HRID84638

反应详情

EQUATION

反应方程式

HRID 84638 的结构方程式

REACTANTS

反应物

3
结构：Nc1ccccc1Cl
HCID7240

2-Chloroaniline

C6H6ClN

结构：O=C(Cl)C(=O)Cl
HCID65578

Ethanedioyl dichloride

C2Cl2O2

结构：O=C(Cl)c1cc2c(s1)-c1cc(Br)ccc1OCC2
HCID86634853

未命名化合物

PRODUCTS

生成物

1
结构：O=C(Nc1ccccc1Cl)c1cc2c(s1)-c1cc(Br)ccc1OCC2
HCID86634852

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Reaction of 2-chloroaniline with 9-bromo-4,5-dihydro-6-oxa-1-thia-benzo[e]azulene-2-carbonyl chloride (prepared from the corresponding carboxylic acid using oxalyl chloride with catalytic N,N-dimethylformamide) yielded 9-bromo-4,5-dihydro-6-oxa-1-thia-benzo[e]azulene-2-carboxylic acid (2-chloro-phenyl)-amide.