huagongshe.com
HRID846665

反应详情

EQUATION

反应方程式

HRID 846665 的结构方程式

REACTANTS

反应物

3
结构：CN(C)C(=O)Cl
HCID6598

Dimethylcarbamoyl chloride

C3H6ClNO

结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：C(#C[C@H]1CCCN1)CN1CCCC1
HCID14730289

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)C(=O)N1CCC[C@H]1C#CCN1CCCC1
HCID54116560

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

This compound was obtained following Example 51, Part A but substituting (S)-1-[3-(2-pyrrolidinyl)-2-propynyl]pyrrolidine for (R)-1-[3-(2-pyrrolidinyl)-2-propynyl]pyrrolidine and dimethyl carbamoyl chloride for acetic anhydride. [α]D -78° (c 1.13, MeOH).

WORKUP

后处理

  1. customThis compound was obtained