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HRID847262

反应详情

EQUATION

反应方程式

HRID 847262 的结构方程式

REACTANTS

反应物

2
结构：O=C1CC(c2cccs2)CN1
HCID11159539

4-(Thiophen-2-yl)pyrrolidin-2-one

C8H9NOS

结构：[Al+3].[H-].[H-].[H-].[H-].[Li+]
HCID21226445

未命名化合物

PRODUCTS

生成物

1
结构：c1csc(C2CCNC2)c1
HCID15029907

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

2 次

PROCEDURE

实验过程

To a suspension of LiAlH4 (0.46 g) in THF (25 ml) was added the product of Example 134 (1.0 g) in THF (30 ml). After the addition was complete the reaction was heated at reflux for 4 hrs.

WORKUP

后处理

  1. additionAfter the addition
  2. temperaturewas heated
  3. temperatureat reflux for 4 hrs