HRID847415

反应详情

EQUATION

反应方程式

HRID 847415 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

350 g of toluene, 135 g of ethyl acrylate, and 15 g of n-decyl methacrylate were polymerized with stirring in a reaction flask at 50°-60° C. under argon with 0.3 g of dodecyl mercaptan as a regulator and 2 g of t-butyl perneodecanoate as initiator. After about 30 minutes of reaction, the mixture was precipitated in methanol and the polymer was dried under vacuum.

WORKUP

后处理

  1. customAfter about 30 minutes of reaction
  2. customthe mixture was precipitated in methanol
  3. customthe polymer was dried under vacuum