HRID850030
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 0 °C
PROCEDURE
实验过程
The product from Step 2 was dissolved in EtOAc at -25° C. and treated with HCl gas until saturated. The reaction was stoppered and stirred at 0° C. for 1 h. Removal of the solvent in vacuo afforded the title compound as a solid.
WORKUP
后处理
- customRemoval of the solvent in vacuo