反应详情

A mixture of 1.1 g. of ethyl 5-hexadecanamido-2-furancarboxylate and 5 ml. of 1 M borane in tetrahydrofuran is refluxed on the steam bath for 3 hours. After cooling, the reaction is poured into dilute hydrochloric acid and the resulting solid filtered. The solid is dissolved in methylene chloride and the solution is filtered through Magnesol. The solvent is evaporated to yield the product.

1. additionA mixture of 1.1 g
2. temperatureAfter cooling
3. filtrationthe resulting solid filtered
4. dissolutionThe solid is dissolved in methylene chloride
5. filtrationthe solution is filtered through Magnesol
6. customThe solvent is evaporated
7. customto yield the product