Diethyl Carbonate → 2-Oxazolidinone, 3-(2-hydroxyethyl)-

HRID 851068Notes

Reaction equation

C(O[C:4](=[O:8])[O:5][CH2:6][CH3:7])C.[NH:9](CCO)[CH2:10][CH2:11][OH:12]>>[OH:12][CH2:11][CH2:10][N:9]1[CH2:7][CH2:6][O:5][C:4]1=[O:8]

Participants

Reactant 2

HCID 7766Diethyl Carbonate

HCID 8113Diethanolamine

Product 1

HCID 768872-Oxazolidinone, 3-(2-hydroxyethyl)-

Procedure

This compound was prepared from diethylcarbonate and diethanolamine in accordance with the method of E. K. Drechsel in the Journal of Organic Chemistry 22 (1957), page 851. A clear, slightly colored liquid having a boiling point of 154° was obtained.

Workup

customwas obtained

Sources & evidence

ORD record: ord-4f654329b3ad4c5abffa5dcda93571c1
Source dataset: uspto-grants-1983_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04382765

Reaction notes

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