反应详情

A mixture of 10 g of 3-(3-methoxyphenyl)-1,2,5,6-tetrahydropyridine hydrochloride, 200 ml of acetone, 14 g of sodium carbonate and 9.3 g of phenacyl bromide were refluxed for 3 hours and was filtered. The filtrate was evaporated to dryness to obtain 14 g of 1-phenyl-2-[3-(3-methoxyphenyl)-1,2,5,6-tetrahydropyridin-1-yl]-ethanone.

1. temperaturewere refluxed for 3 hours
2. filtrationwas filtered
3. customThe filtrate was evaporated to dryness