huagongshe.com
HRID855780

反应详情

EQUATION

反应方程式

HRID 855780 的结构方程式

REACTANTS

反应物

5
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：On1nnc2ccccc21
HCID75771

1-Hydroxybenzotriazole

C6H5N3O

结构：CN(CC(=O)O)C(=O)OC(C)(C)C
HCID83692

Glycine, N-[(1,1-dimethylethoxy)carbonyl]-N-methyl-

C8H15NO4

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[B-](F)(F)F
HCID2733207

O-(Benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate

C11H16BF4N5O

结构：CCOC(=O)c1cc2cc(N)ccc2o1
HCID9837138

Ethyl 5-aminobenzofuran-2-carboxylate

C11H11NO3

PRODUCTS

生成物

1
结构：CCOC(=O)c1cc2cc(NC(=O)CNCC(=O)OC(C)(C)C)ccc2o1
HCID69145149

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

50 ml of DMF are added to 0.95 g of Boc-sarcosine and 1.21 g of ethyl 5-aminobenzofuran-2-carboxylate. 1.77 g of TBTU and 0.23 g of HOBt are then added, and the mixture is neutralised using 4 ml of triethylamine. The mixture is stirred overnight at room temperature.