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HRID863238

反应详情

EQUATION

反应方程式

HRID 863238 的结构方程式

REACTANTS

反应物

4
结构：CS(C)=O
HCID679

Dimethyl sulfoxide

C2H6OS

结构：O=C(Cl)C(=O)Cl
HCID65578

Ethanedioyl dichloride

C2Cl2O2

结构：CC(C)(CCOCc1ccccc1)C[C@@H](CO)NC(=O)OC(C)(C)C
HCID22882578

未命名化合物

结构：CCCCNC(=O)[C@H](C)C[C@H](O)[C@H](CC(C)(C)CC(=O)N1CC(C(=O)OCC)Cc2ccccc21)NC(=O)OC(C)(C)C
HCID131720511

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(CCOCc1ccccc1)C[C@@H](C=O)NC(=O)OC(C)(C)C
HCID22882579

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

The title compound is prepared starting from 28.1 g of 6-benzyloxy-2(S)-tert-butoxycarbonylamino-4,4-dimethyl-hexan-1-ol, 10.5 ml of oxalyl chloride, 11.4 ml of dimethyl sulfoxide and 45 ml of triethylamine analogously to Example 1g): Rf (A)=0.62; Rt (I)=28.1 min; FAB-MS: (M+H)+ =350.