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HRID873830

反应详情

EQUATION

反应方程式

HRID 873830 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(CN)cc1
HCID75452

4-Methoxybenzylamine

C8H11NO

结构：CCOC(=O)c1nn(C)c(C)c1C(O)c1ccc(Cl)cc1
HCID117702851

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1nn(C)c(C)c1C(NCc1ccc(OC)cc1)c1ccc(Cl)cc1
HCID117702748

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 1.4 using ethyl 4-((4-chlorophenyl)(hydroxy)methyl)-1,5-dimethyl-1H-pyrazole-3-carboxylate (Step 25.2) and 4-methoxybenzylamine. tR: 3.99 min (HPLC 1); tR: 0.86 min (LC-MS 2); ESI-MS: 428 [M+H]+ (LC-MS 2); Rf=0.59 (EtOAc).