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HRID873907

反应详情

EQUATION

反应方程式

HRID 873907 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccc(Cl)cc1
HCID7726

4-Chlorobenzaldehyde

C7H5ClO

结构：CCOC(=O)C(=O)CC(C)=O
HCID69208

Ethyl 2,4-dioxovalerate

C7H10O4

结构：Cn1cc(N)cc(Cl)c1=O
HCID71756073

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)C1=C(O)C(=O)N(c2cc(Cl)c(=O)n(C)c2)C1c1ccc(Cl)cc1
HCID117702763

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 57.1 using 5-amino-3-chloro-1-methylpyridin-2(1H)-one (Step 5.2), 4-chlorobenzaldehyde and ethyl 2,4-dioxovalerate at 120° C. for 1 hr. tR: 3.73 min (HPLC 1); tR: 0.74 min (LC-MS 2); ESI-MS: 393/395 [M+H]+ (LC-MS 2).