huagongshe.com
HRID873923

反应详情

EQUATION

反应方程式

HRID 873923 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccc(Cl)cc1
HCID7726

4-Chlorobenzaldehyde

C7H5ClO

结构：CCOC(=O)C(=O)CC(=O)CC
HCID61590

Ethyl 2,4-dioxohexanoate

C8H12O4

结构：Cc1cc(N)cn2c(C)nnc12
HCID75357449

未命名化合物

PRODUCTS

生成物

1
结构：CCC(=O)C1C(=O)C(=O)N(c2cc(C)c3nnc(C)n3c2)C1c1ccc(Cl)cc1
HCID117702535

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 60.1 using 3,8-dimethyl-[1,2,4]triazolo[4,3-a]pyridin-6-amine (Step 67.4), 4-chlorobenzaldehyde and ethyl 2,4-dioxohexanoate at 110° C. for 4 hr. tR: 0.79 min (LC-MS 2); ESI-MS: 411 [M+H]+, ESI-MS: 409 [M−H]− (LC-MS 2).