反应详情

The mixture of 2-bromo-1-fluoro-4-nitrobenzene (5 g), (3-fluorophenyl)methanol (2.86 g) and K2CO3 (9.4 g) in Acetone (50 mL) was refluxed for 4 h. The solid was filtered and the solvent was removed. The obtained yellow solid was recrystallized from EtOAc/Hexane to provide brown solid (6.8 g). Yield: 92%.

1. temperaturewas refluxed for 4 h
2. filtrationThe solid was filtered
3. customthe solvent was removed
4. customThe obtained yellow solid was recrystallized from EtOAc/Hexane