HRID889265

反应详情

EQUATION

反应方程式

HRID 889265 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
0 °C

PROCEDURE

实验过程

To a solution of 2,2-dimethyl-pent-4-enoic acid (500 mg, 3.0 mmol) in THF (4 mL) is added 9-BBN (0.5M, 17 mL, 3.0 mmol) at 0° C. and it is stirred at 0° C. for 2 h. The solvent is removed via vacuum to give the title compound and it is used directly in the next step.

WORKUP

后处理

  1. customThe solvent is removed via vacuum