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HRID893234

反应详情

EQUATION

反应方程式

HRID 893234 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CNc1ccc(Br)cc1
HCID2757052

Benzenamine, 4-bromo-N-methyl-

C7H8BrN

结构：CCOC(=O)C1(C(=O)Cl)CC1
HCID14233946

Ethyl 1-(chlorocarbonyl)cyclopropanecarboxylate

C7H9ClO3

PRODUCTS

生成物

1
结构：CCOC(=O)C1(C(=O)N(C)c2ccc(Br)cc2)CC1
HCID19096870

未命名化合物

收率 50%

PROCEDURE

实验过程

Ethyl 1-chlorocarbonylcyclopropanecarboxylate (3.11 grams, 0.02 mole), prepared in Example XVIII, 4-bromo-N-methylaniline (3.00 grams, 0.02 mole) and triethylamine (1.63 grams, 0.02 mole) were reacted in a manner similar to that described in Example III to give 3.79 grams (0.01 mole) of ethyl 1-[N-(4-bromophenyl)-N-methylaminocarbonyl]cyclopropanecarboxylate isolated as a colorless oil.

WORKUP

后处理

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