Sodium ethoxide → HCID 86737913, compound

HRID 894081Notes

Reaction equation

HRID 894081 reaction equation
[C:1]1([C:7]2[NH:11][CH:10]=[C:9]([C:12]([O-:14])=[S:13])[CH:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[O-]CC.[Na+:18]>C(OCC)(=O)C>[C:1]1([C:7]2[NH:11][CH:10]=[C:9]([C:12]([O-:14])=[S:13])[CH:8]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1.[Na+:18]

Participants

4

Reactant 2

HCID 2723922Sodium ethoxideHCID 178526149HCID 178526149, compound

Product 1

HCID 86737913HCID 86737913, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

5-Phenylthiopyrrole-3-carboxylate is combined with an equivalent of sodium ethoxide in ethyl acetate. Sodium 5-phenylthiopyrrole-3-carboxylate is isolated by concentration to dryness or by precipitation resulting from addition of a non-solvent (ether or hexane).

Sources & evidence

ORD record
ord-7f8b8217df0b4574b2c43145fa4976f2
Source dataset
uspto-grants-1981_08
Patent number
US04282242

Reaction notes

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