Azobisisobutyronitrile → N-vinylpyrrolidone N-methacryloyl D-glucosamine

HRID 894305Notes

Reaction equation

HRID 894305 reaction equation
[Pb].[N].[CH:3]([N:5]1[CH2:9][CH2:8][CH2:7][C:6]1=[O:10])=[CH2:4].[C:11]([NH:16][C@@H:17]1[C@@H:23]([OH:24])[C@H:22]([OH:25])[C@@H:21]([CH2:26][OH:27])[O:20][CH:18]1[OH:19])(=[O:15])[C:12]([CH3:14])=[CH2:13].N(C(C)(C)C#N)=NC(C)(C)C#N>C(O)C>[CH:3]([N:5]1[CH2:9][CH2:8][CH2:7][C:6]1=[O:10])=[CH2:4].[C:11]([NH:16][C@@H:17]1[C@@H:23]([OH:24])[C@H:22]([OH:25])[C@@H:21]([CH2:26][OH:27])[O:20][CH:18]1[OH:19])(=[O:15])[C:12]([CH3:14])=[CH2:13]

Participants

6

Reactant 4

HCID 6547AzobisisobutyronitrileHCID 6917N-vinyl-2-pyrrolidoneHCID 15756262N-methacryloyl D-glucosamineHCID 178514658HCID 178514658, compound

Product 1

HCID 86737931N-vinylpyrrolidone N-methacryloyl D-glucosamine

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Into a 500 ml round bottom flask fitted with a stirrer and a nitrogen lead-in tube, 100 g of ethanol, 95 g of distilled N-vinylpyrrolidone, 5 g of N-methacryloyl D-glucosamine and 1 g of azo-bisisobutyronitrile are introduced.

Workup

  1. customInto a 500 ml round bottom flask fitted with a stirrer

Sources & evidence

ORD record
ord-2dcea020f5f449de82f6f8b53bdb17bf
Source dataset
uspto-grants-1981_08
Patent number
US04283384

Reaction notes

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