HRID894306

反应详情

EQUATION

反应方程式

HRID 894306 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
30 °C

PROCEDURE

实验过程

Into a 2 liter round bottom flask 800 ml of ethanol, 12.8 g of sodium hydroxide pellets and 80 g of a copolymer composed of 70% N-vinylpyrrolidone and 30% vinyl acetate are introduced. The resulting reaction mixture is maintained with stirring at 30° C. for 2 hours and is then poured into 8 liters of diethyl ether to precipitate the desired polymer. After filtration the polymer is dried under reduced pressure. Yield: 95%.

WORKUP

后处理

  1. additionare introduced
  2. customThe resulting reaction mixture
  3. temperatureis maintained
  4. customto precipitate the desired polymer
  5. filtrationAfter filtration the polymer
  6. customis dried under reduced pressure