1-Methylcyclohexanecarboxylic acid → HCID 23710569, compound

HRID 894363Notes

Reaction equation

HRID 894363 reaction equation
[CH3:1][C:2]1([C:8]([OH:10])=[O:9])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.C[O-].[Na+:13].[Na]>CO>[CH3:1][C:2]1([C:8]([O-:10])=[O:9])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.[Na+:13]

Participants

5

Reactant 3

HCID 707441-Methylcyclohexanecarboxylic acidHCID 5360545SodiumHCID 10942334Sodium Methoxide

Product 1

HCID 23710569HCID 23710569, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent3×

Conditions

Temperature
50 °C

Procedure

0.1 mole of 1-methyl-1-cyclohexyl-carboxylic acid prepared by a method similar to that used in example 7, dissolved in methanol was added to a solution of sodium methylate in dry methanol, prepared using 0.095 mole of sodium and 40 cm3 of methanol as the starting materials. The mixture was heated at 50° C. for 10 minutes and the methanol was then evaporated off in vacuo. The colourless crystals of sodium 1-methyl-1-cyclohexyl-carboxylate were washed with ether, filtered off and dried.

Workup

  1. customprepared
  2. customthe methanol was then evaporated off in vacuo
  3. washThe colourless crystals of sodium 1-methyl-1-cyclohexyl-carboxylate were washed with ether
  4. filtrationfiltered off
  5. customdried

Sources & evidence

ORD record
ord-cd7c346832b84ce09cc4413ee59f8c74
Source dataset
uspto-grants-1981_08
Patent number
US04283420

Reaction notes

Loading…