Hydrochloric Acid → HCID 13881503, compound

HRID 894593Notes

Reaction equation

HRID 894593 reaction equation
[CH3:1][C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[C:4]([CH3:9])[C:3]=1[NH:10][CH2:11][CH:12]([NH:14][C:15]1[C:20]([CH3:21])=[CH:19][CH:18]=[CH:17][C:16]=1[CH3:22])[CH3:13].ClC(C)[CH2:25][NH:26]C1C(C)=CC(C)=CC=1C.CC1C=CC=C(C)C=1N.Cl>>[CH3:1][C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[C:4]([CH3:9])[C:3]=1[N:10]1[CH2:11][CH:12]([CH3:13])[N:14]([C:15]2[C:20]([CH3:21])=[CH:19][CH:18]=[CH:17][C:16]=2[CH3:22])[C:25]1=[NH:26]

Participants

5

Reactant 4

HCID 313Hydrochloric AcidHCID 68962,6-DimethylanilineHCID 20512417HCID 20512417, compoundHCID 20512433HCID 20512433, compound

Product 1

HCID 13881503HCID 13881503, compoundYield 65.6%

Procedure

1-(2',4',6'-Trimethylphenyl-amino)-2-(2',6'-dimethylphenyl-amino)-propane, applied as starting substance, is obtained with a yield of 65.6% by reacting N-(β-chloropropyl)-2,4,6-trimethyl-aniline, a compound prepared according to Example 16, point (b), with 2,6-dimethylaniline under the conditions given in Example 16, point (c). The hydrochloride of the product melts at 174°-177° C.

Workup

  1. customis obtained with a yield of 65.6%
  2. customa compound prepared

Sources & evidence

ORD record
ord-635f6d3e577e4701b6532f64da0a217d
Source dataset
uspto-grants-1981_08
Patent number
US04284642

Reaction notes

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