Methyl Acrylate → HCID 11206303, compound

HRID 895311Notes

Reaction equation

HRID 895311 reaction equation
[C:1]([O:5][CH3:6])(=[O:4])[CH:2]=[CH2:3].[NH:7]([CH2:11][CH2:12][OH:13])[CH2:8][CH2:9][OH:10]>>[OH:10][CH2:9][CH2:8][N:7]([CH2:3][CH2:2][C:1]([O:5][CH3:6])=[O:4])[CH2:11][CH2:12][OH:13]

Participants

3

Reactant 2

HCID 7294Methyl AcrylateHCID 8113Diethanolamine

Product 1

HCID 11206303HCID 11206303, compoundYield 98%

Procedure

At 20 to 30° C., 9.01 g of methyl acrylate was added to 10.0 g of diethanolamine. The resulting mixture was allowed to stand for 20 hours. The reaction mixture was concentrated under reduced pressure, whereby N,N-bis(2-hydroxyethyl)-2-(methoxycarbonyl)ethylamine was obtained (yield: 98%).

Workup

  1. concentrationThe reaction mixture was concentrated under reduced pressure

Sources & evidence

ORD record
ord-82a7241fc05e4cd98854a47268709c2e
Source dataset
uspto-grants-2005_07
Patent number
US06916593B2

Reaction notes

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