Hydrochloric Acid → HCID 22346282, compound

HRID 897345Notes

Reaction equation

HRID 897345 reaction equation
[CH:1]([S:3]([NH:6][CH2:7][CH2:8][NH:9]C(=O)OC(C)(C)C)(=[O:5])=[O:4])=[CH2:2].[ClH:17]>CCOC(C)=O>[Cl-:17].[CH:1]([S:3]([NH:6][CH2:7][CH2:8][NH3+:9])(=[O:5])=[O:4])=[CH2:2]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22346254HCID 22346254, compound

Product 1

HCID 22346282HCID 22346282, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

A solution of tert-butyl 2-[(vinylsulfonyl)amino]ethylcarbamate (1.60 g, 6.39 mmol) in EtOAc (55 ml) at 0 C, was saturated with HCl gas and then stirred for 1 hr. The solvent was evaporated in vacuo to afford the product as a viscous oil.

Workup

  1. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-8111952135b1401e927496d71ea38cf9
Source dataset
uspto-grants-2005_07
Patent number
US06921759B2

Reaction notes

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