反应详情

To a solution of N-methyl-1,3-diaminopropane (37.6 mL, 312 mmol) and sulfamide (10.0 g, 104 mmol) were heated at reflux for 16 hr. The solvent was evaporated in vacuo and the residue was purified by chromatography (SiO2, EtOAc/CH2Cl2: 1:1) to afford the title compound as an oil.

1. temperatureat reflux for 16 hr
2. customThe solvent was evaporated in vacuo
3. customthe residue was purified by chromatography (SiO2, EtOAc/CH2Cl2: 1:1)