Pyridine-2-carbonitrile → HCID 178426508, compound

HRID 901921Notes

Reaction equation

HRID 901921 reaction equation
[C:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][N:4]=1)#[N:2].[CH3:9][C:10]1[CH:16]=[CH:15][C:13]([NH2:14])=[CH:12][CH:11]=1>>[CH3:9][C:10]1[CH:16]=[CH:15][C:13]([NH:14][C:1]([C:3]2[CH:8]=[CH:7][CH:6]=[CH:5][N:4]=2)=[NH:2])=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 7522Pyridine-2-carbonitrileHCID 7813p-Toluidine

Product 1

HCID 178426508HCID 178426508, compound

Procedure

The title compound was prepared from 2-cyanopyridine (9.7 g, 93 mmol) and 4-methylaniline (10 g, 93 mmol) by following the procedure described in preparation 10 (8.2 g, yield 41.6%). MS m/z:212.1(M+).

Sources & evidence

ORD record
ord-9b22b2fd17ae4aa3b5b9767931cdb5ff
Source dataset
uspto-grants-2008_04
Patent number
US07365069B2

Reaction notes

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