1-Methylpiperazine → HCID 136335630, compound

HRID 903096Notes

Reaction equation

HRID 903096 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[N:11]=[C:10]([C:12]([N+:15]([O-:17])=O)=[N:13]O)[CH2:9][N:8]=[C:7]([C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=3[F:24])[C:6]=2[CH:25]=1.[CH3:26][N:27]1[CH2:32][CH2:31]N[CH2:29][CH2:28]1>O1CCCC1>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[N:11]=[C:10]([C:12]([N:13]3[CH2:31][CH2:32][N:27]([CH3:26])[CH2:28][CH2:29]3)=[N:15][OH:17])[CH2:9][N:8]=[C:7]([C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][C:19]=3[F:24])[C:6]=2[CH:25]=1

Participants

4

Reactant 2

HCID 531671-MethylpiperazineHCID 136335629HCID 136335629, compound

Product 1

HCID 136335630HCID 136335630, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

This compound was obtained by reacting 7-chloro-5-(2-fluorophenyl)-N-hydroxy-α-nitro-3H-1,4-benzodiazepine-2-methanimine with N-methylpiperazine in tetrahydrofuran. The analytical sample was recrystallized from ethanol, mp 198°-200° C.

Workup

  1. customThis compound was obtained
  2. customThe analytical sample was recrystallized from ethanol, mp 198°-200° C.

Sources & evidence

ORD record
ord-8b4abc12ca9b47e5b40d340aed555851
Source dataset
uspto-grants-1980_10
Patent number
US04226768

Reaction notes

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