HRID903818

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID73696

Propanedinitrile, 2,2'-(1,4-cyclohexanediylidene)bis-

C12H8N4

PRODUCTS

生成物

HCID73697

Propanedinitrile, 2,2'-(2,5-cyclohexadiene-1,4-diylidene)bis-

C12H4N4

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID178418406

未命名化合物

溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

According to the procedure of Fatiadi Synthesis, 1976, 133, incorporated herein by reference, the 1,4-bis(dicyanomethylene)cyclohexane is allowed to react with manganese dioxide in refluxing (110° C.) toluene for ca. 15 minutes to provide TCNQ in ca. 60% yields.

WORKUP

后处理

customAccording to the procedure of Fatiadi Synthesis, 1976, 133