Hydrochloric Acid → HCID 3068096, compound

HRID 905131Notes

Reaction equation

HRID 905131 reaction equation
[C:1]([C:4]1[CH:5]=[C:6]([CH:12]=[CH:13][CH:14]=1)[CH:7]=[CH:8][C:9]([OH:11])=[O:10])(=[O:3])[CH3:2].[Cl:15][C:16]1[CH:23]=[CH:22][C:19]([CH:20]=O)=[CH:18][CH:17]=1.Cl.[CH2:25](O)[CH3:26]>>[Cl:15][C:16]1[CH:23]=[CH:22][C:19]([CH:20]=[CH:2][C:1]([C:4]2[CH:5]=[C:6]([CH:12]=[CH:13][CH:14]=2)[CH:7]=[CH:8][C:9]([O:11][CH2:25][CH3:26])=[O:10])=[O:3])=[CH:18][CH:17]=1

Participants

5

Reactant 4

HCID 313Hydrochloric AcidHCID 702Ethanol2×HCID 77264-ChlorobenzaldehydeHCID 54265267HCID 54265267, compound

Product 1

HCID 3068096HCID 3068096, compound

Procedure

12 g (0.055 mole) of the ethyl ester of 3-acetyl-cinnamic acid are dissolved in 120 ml of ethanol. 8 g (0.057 mole) of para-chlorobenzaldehyde are added then 35 ml of anhydrous ethanol saturated with gaseous hydrochloric acid. The reaction medium is stirred for 10 hours.

Sources & evidence

ORD record
ord-d0c7ecba6af441a69e55fe399d9465f9
Source dataset
uspto-grants-1983_12
Patent number
US04421927

Reaction notes

Loading…