Trifluoroacetic acid → HCID 87119124, compound

HRID 905497Notes

Reaction equation

HRID 905497 reaction equation
O.[NH2:2][NH2:3].[F:4][C:5]([F:10])([F:9])[C:6]([OH:8])=[O:7]>O>[O-:8][C:6]([C:5]([F:10])([F:9])[F:4])=[O:7].[NH3+:2][NH2:3]

Participants

4

Reactant 2

HCID 6422Trifluoroacetic acidHCID 24654Hydrazine hydrate (1:1)

Product 1

HCID 87119124HCID 87119124, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Hydrazine monohydrate (4.41 ml, 90.9 mmol) was added via syringe to a 250-ml round-bottom flask containing 50 ml of distilled water with stirring at room temperature. Trifluoroacetic acid (7.0 ml, 90.9 mmol) was added via syringe and the reaction was stirred at room temperature overnight. The water was removed in vacuo with heating to 80° C., yielding product as a colorless liquid.

Workup

  1. stirringthe reaction was stirred at room temperature overnight
  2. customThe water was removed in vacuo
  3. temperaturewith heating to 80° C.
  4. customyielding product as a colorless liquid

Sources & evidence

ORD record
ord-2a7b2e65539648518a3582a62347c242
Source dataset
uspto-grants-2011_09
Patent number
US08012277B2

Reaction notes

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