HRID905504

反应详情

EQUATION

反应方程式

HRID 905504 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

3,5-Diamino-1,2,4-triazole (1.50 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

WORKUP

后处理

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C. for 4 hours